glyoxylic acid tert-butyl ester in toluene 1 h; Ambient temperature;
参考文献
Ramage, Robert; McCleery, Patrick P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1555 - 1560
1: 65 percent / toluene / 1 h / Heating 2: NaOH / H2O; tetrahydrofuran / 18 h / Ambient temperature 3: 73 percent / toluene-p-sulphonic acid hydrate / toluene / 9 h / Heating View Scheme
参考文献
Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537
Ramage, Robert; McCleery, Patrick P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1555 - 1560
1: 65 percent / toluene / 1 h / Heating 2: NaOH / H2O; tetrahydrofuran / 18 h / Ambient temperature View Scheme
参考文献
Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537
Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537
1: N-bromosuccinimide, azobisisobutyronitrile / CCl4 / 0.5 h / Heating; Irradiation
2: 79 percent / toluene / 20 °C
3: 1,4-diazabicyclo<2.2.2>octane / benzene / 0.07 h / Ambient temperature
View Scheme
参考文献
Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537
1: 79 percent / toluene / 20 °C
2: 1,4-diazabicyclo<2.2.2>octane / benzene / 0.07 h / Ambient temperature
View Scheme
参考文献
Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537