2,4,6-三甲基苯甲酰氯合成路线 (共 72 条)
反应条件
T=20°C; 2 h; Inert atmosphere;
参考文献
Przychodzen, Witold; Nycz, Jacek E.; Nam, Young-Joo; Lee, Dong-Ung
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 10 p. 3098 - 3100
参考文献
Kharasch; Morrison; Urry
Journal of the American Chemical Society, 1944 , vol. 66, p. 368,370
参考文献
Kharasch; Morrison; Urry
Journal of the American Chemical Society, 1944 , vol. 66, p. 368,370
反应条件
1: benzene 2: 190 °C View Scheme
参考文献
Furukawa,N. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 3599 - 3605
反应条件
N,N-dimethyl-cyclohexylamine T=80 - 85°C; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2004/87723 A2, 2004 ;
Location in patent: Page/Page column 12-14 ;
参考文献
Kohler, Baltzly
Journal of the American Chemical Society, 1932 , vol. 54, p. 4015,4022
Full Text Show Details
Nauta; Wuis
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 535,540
Full Text Show Details
Coops et al.
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 1109,1111
反应条件
1: pyridine / 150 °C 2: diethyl ether; benzene View Scheme
参考文献
Fuson; Corse; Rabjohn
Journal of the American Chemical Society, 1941 , vol. 63, p. 2852
反应条件
aluminium trichloride
参考文献
Holm, Torkil
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 4 p. 266 - 268
反应条件
1: diethyl ether 2: sodium-amalgam; ethanol 3: red phosphorus; aqueous HI View Scheme
参考文献
Kohler, Baltzly
Journal of the American Chemical Society, 1932 , vol. 54, p. 4015,4022
反应条件
1: 59 percent / 3 h / Ambient temperature 2: 43 percent / HN3, H2SO4 / CHCl3 / 20 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 116, # 3 p. 1016 - 1026