2,4-二甲基-1-(三氟甲基)苯合成路线 (共 9 条)
反应条件
copper(l) iodide in 1-methyl-pyrrolidin-2-one
T=160°C;
参考文献
DeCosta, Dayal; Pincock, James
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9484 - 9487
反应条件
potassium fluoride; silver trifluoromethanesulfonate in 1,2-dichloro-ethane
T=85°C; 24 h; Inert atmosphereDarkness;
参考文献
Ye, Yingda; Lee, Shin Hee; Sanford, Melanie S.
Organic Letters, 2011 , vol. 13, # 20 p. 5464 - 5467
参考文献
Solvay Interox Limited
Patent: US5557008 A1, 1996 ;
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide
T=23 - 50°C; 42 h; GloveboxSealed tube;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
反应条件
in acetonitrile
8.33333 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
DeCosta, Dayal; Pincock, James
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9484 - 9487
反应条件
in acetonitrile
2.16667 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
DeCosta, Dayal; Pincock, James
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9484 - 9487
反应条件
in acetonitrile
0.5 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
DeCosta, Dayal; Pincock, James
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9484 - 9487
反应条件
in acetonitrile
0.5 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
DeCosta, Dayal; Pincock, James
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9484 - 9487
反应条件
in acetonitrile
0.5 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
DeCosta, Dayal; Pincock, James
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9484 - 9487