in neat (no solvent)
byproducts: Cl2; react. with NO2 in a sealing tube at 200-250 °C; formation of N2O, N2, Cl2, NOCl, NO2Cl and a compound with composition P4O12N;;
in not given
byproducts: N4P4F4Cl4; react. of (NPCl2)3 with PbF2;; freezing out, dissolving in petroleum ether; fractionation, at 50 °C (NPF2)3, at 70-95 °C (NPF2)4;;
in tetrahydrofuran
9 h; Heating; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mitropol'skaya, G. I.; Kireev, V. V.; Korshak, V. V.; Goryaev, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 11 p. 2486 - 2491,2197 - 2201
Gol'din, G. S.; Fedorov, S. G.; Kotova, E. V.; Bochkarev, V. N.; Slyusarenko, T. F.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 1 p. 21 - 23,15 - 17
pyridine in nitrobenzene
T=90 - 95°C; 5 h; various initial molar ratios of reagents; various reaction times.; Product distribution;
参考文献
Gol'din, G. S.; Fedorov, S. G.; Kotova, E. V.; Bochkarev, V. N.; Slyusarenko, T. F.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 1 p. 21 - 23,15 - 17
