1，1-二氯-2，2-双(4-氯苯基)乙烯合成路线 （共 5 条）
反应条件
4-(N,N-dimethlyamino)pyridine; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in N,N-dimethyl-formamide
参考文献
US2014/134110 A1, ;
Paragraph 0155; 0156 ;
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in N,N-dimethyl-formamide
参考文献
Demmer; Dijkgraaf; Schottelius; Wester; Kessler
Organic Letters, 2008 , vol. 10, # 10 p. 2015 - 2018
参考文献
Simerska, Pavla; Christie, Michelle P.; Goodwin, Daryn; Jen, Freda E.-C.; Jennings, Michael P.; Toth, Istvan
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 97, p. 196 - 202
反应条件
1: α-Fmoc-L-lysine hydrochloride With N-ethyl-N,N-diisopropylamine in water T=20°C; 2: Dde-OH With trifluoroacetic acid in ethanol; water 60 h; Reflux;
参考文献
Walton, Tashfeen; Bradley, Mark; Dhaliwal, Kev; Avlonitis, Nikolaos; Haslett, Chris; McDonald, Neil; Debunne, Manuelle
Patent: US2014/134110 A1, 2014 ;
Location in patent: Paragraph 0155; 0157 ;
反应条件
trifluoroacetic acid in ethanol 60 h; Heating;
参考文献
Chhabra, Siri Ram; Hothi, Bhupinder; Evans, David J.; White, Peter D.; Bycroft, Barrie W.; Chan, Weng C.
Tetrahedron Letters, 1998 , vol. 39, # 12 p. 1603 - 1606
