2-巯基-S-硫代苯甲酰乙酸合成路线 （共 56 条）
反应条件
sodium hydroxide; hydrazine hydrate
pH=5 - 6; 1 h; cooling;
参考文献
Kalinowski, Danuta S.; Sharpe, Philip C.; Bernhardt, Paul V.; Richardson, Des R.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 24 p. 6212 - 6225
参考文献
Chen, Shoujun; Sun, Lijun; Koya, Keizo; Tatsuta, Noriaki; Xia, Zhiqiang; Korbut, Timothy; Du, Zhenjian; Wu, Jim; Liang, Guiqing; Jiang, Jun; Ono, Mitsunori; Zhou, Dan; Sonderfan, Andrew
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 18 p. 5070 - 5076
参考文献
Holmberg
Arkiv foer Kemi, 1944 , vol. 17 A, # 23 p. 2,3
参考文献
Leon,N.H.; Asquith,R.S.
Tetrahedron, 1970 , vol. 26, p. 1719 - 1725
参考文献
Lawson; Searle
Journal of the Chemical Society, 1957 , p. 1556,1561
Full Text Show Details
Holmberg
Arkiv foer Kemi, 1947 , vol. 24A, # 3 p. 16
反应条件
1: 76 percent / 1.) 76percent NaOH, 2.) AcOH / 1.) H2O, room temp., 10 min, 2.) 0 deg C
2: 50 percent / pyridine / 4 h
View Scheme
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
反应条件
sodium hydroxide in water
Ambient temperature;
参考文献
Kurzer, Frederic; Secker, Jane L.
Tetrahedron, 1981 , vol. 37, p. 1429 - 1436
反应条件
sodium hydroxide
1.5 h; Ambient temperature;
参考文献
Kurzer, Frederick; Doyle, Kevin M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1873 - 1880
参考文献
Holmberg
Arkiv foer Kemi, 1947 , vol. 24A, # 3 p. 16
反应条件
1: With sodium hydroxide in water
T=0 - 10°C;
2: in water
T=0 - 5°C; 0.5 h;
参考文献
Yadav, Arun A.; Patel, Daywin; Wu, Xing; Hasinoff, Brian B.
Journal of Inorganic Biochemistry, 2013 , vol. 126, p. 1 - 6
