N-(4-乙酰基巯基苯基)乙酰胺合成路线 （共 19 条）
反应条件
1: aq.-ethanolic NaOH 3: aqueous H2O2 View Scheme
参考文献
Baker et al.
Journal of Organic Chemistry, 1950 , vol. 15, p. 400
参考文献
Journal of Organic Chemistry, , vol. 15, p. 400
反应条件
water T=25°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 99, p. 451 - 464
反应条件
1: aq.-ethanolic NaOH 3: aqueous H2O2 4: Raney nickel; 1-ethoxy-ethanol-(2) / Hydrogenation 5: aqueous hydrochloric acid View Scheme
参考文献
Baker et al.
Journal of Organic Chemistry, 1950 , vol. 15, p. 400
反应条件
potassium hydroxide in water; ethylene glycol
参考文献
Hoechst Celanese Corporation
Patent: US5157142 A1, 1992 ;
反应条件
1: N-(4-bromo-phenyl)-acetamide With tris-(dibenzylideneacetone)dipalladium(0); Josiphos-CyPF-t-Bu in toluene
T=20°C; 0.0833333 h; Inert atmosphere;
2: thiolacetic acid potassium salt in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Van Den Hoogenband, Adri; Lange, Jos H. M.; Bronger, Raymond P. J.; Stoit, Axel R.; Terpstra, Jan Willem
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6877 - 6881
反应条件
copper(l) iodide; 1,10-phenanthroline in toluene
T=100°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Soria-Castro, Silvia M.; Penenory, Alicia B.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 467 - 475
反应条件
N,N'-dimethyl-N,N'-di(pyridin-4-yl)ferrocene-1,1'-dicarboxamide
T=20°C; 0.583333 h;
参考文献
Kashyap, Bishwapran; Phukan, Prodeep
RSC Advances, 2013 , vol. 3, # 35 p. 15327 - 15336
反应条件
1: C7H6BrNO With tris-(dibenzylideneacetone)dipalladium(0); Josiphos-CyPF-t-Bu in toluene
T=20°C; 0.0833333 h; Inert atmosphere;
2: thiolacetic acid potassium salt in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Van Den Hoogenband, Adri; Lange, Jos H. M.; Bronger, Raymond P. J.; Stoit, Axel R.; Terpstra, Jan Willem
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6877 - 6881
参考文献
Hupe,D.J.; Jencks,W.P.
Journal of the American Chemical Society, 1977 , vol. 99, p. 451 - 464
