反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C 1.2: 2 h / -78 °C 2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -20 °C 3.1: n-butyllithium / tetrahydrofuran; hexane; toluene / 0.17 h / -78 °C 3.2: 2 h / -78 °C 4.1: C6HMe5; boron trichloride / n-heptane; dichloromethane / 4 h / -78 °C 4.2: -78 - 20 °C View Scheme
参考文献
Imamura, Masakazu; Nakanishi, Keita; Suzuki, Takayuki; Ikegai, Kazuhiro; Shiraki, Ryota; Ogiyama, Takashi; Murakami, Takeshi; Kurosaki, Eiji; Noda, Atsushi; Kobayashi, Yoshinori; Yokota, Masayuki; Koide, Tomokazu; Kosakai, Kazuhiro; Ohkura, Yasufumi; Takeuchi, Makoto; Tomiyama, Hiroshi; Ohta, Mitsuaki
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 10 p. 3263 - 3279
