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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并噻唑
合成路线
（共 604 条）
95-16-9
苯并噻唑
+
100-53-8
苄硫醇
→
反应条件
19654-17-2
反应条件
copper diacetate; silver trifluoroacetate in N,N-dimethyl-formamide T=120°C; 12 h; Inert atmosphere;
参考文献
Dai, Chao; Xu, Zhaoqing; Huang, Fei; Yu, Zhengkun; Gao, Yan-Feng
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4414 - 4419
95-16-9
苯并噻唑
+
1878-67-7
3-溴苯乙酸
→
反应条件
19654-14-9
2-(3-溴苯基)苯并[d]噻唑
反应条件
oxygen; copper diacetate in dimethyl sulfoxide T=130°C; 26 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
95-16-9
苯并噻唑
+
2039-86-3
间溴苯乙烯
→
反应条件
19654-14-9
2-(3-溴苯基)苯并[d]噻唑
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
95-16-9
苯并噻唑
+
1300105-80-9
→
反应条件
615-22-5
2-甲硫基苯并噻唑
+
2040-20-2
p-甲氧基异苯丁酮
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; dimethyl-disulfide; 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran T=90°C; 3 h; Inert atmosphere;
参考文献
Arisawa, Mieko; Toriyama, Fumihiko; Yamaguchi, Masahiko
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
+
586-77-6
→
反应条件
10205-56-8
反应条件
sodium hydroxide; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; [(t-Bu)3PH]BF4 in dimethyl sulfoxide T=60°C; 24 h;
参考文献
Miyaoku, Takayuki; Mori, Atsunori
Heterocycles, 2009 , vol. 77, # 1 p. 151 - 155
95-16-9
苯并噻唑
+
100-10-7
→
反应条件
10205-56-8
反应条件
iron sulphate heptahydrate; oxygen in diethylene glycol dimethyl ether; water T=150°C; 20 h; Sealed tube;
参考文献
Liu, Saiwen; Chen, Ru; Guo, Xiangyu; Yang, Huiqiong; Deng, Guojun; Li, Chao-Jun
Green Chemistry, 2012 , vol. 14, # 6 p. 1577 - 1580
95-16-9
苯并噻唑
+
79-31-2
→
反应条件
17626-86-7
反应条件
dipotassium peroxodisulfate; silver nitrate in dichloromethane; water T=20°C; 8 h;
参考文献
Zhao, Wei-Ming; Chen, Xiao-Lan; Yuan, Jin-Wei; Qu, Ling-Bo; Duan, Li-Kun; Zhao, Yu-Fen
Chemical Communications, 2014 , vol. 50, # 16 p. 2018 - 2020
95-16-9
苯并噻唑
+
75-30-9
→
反应条件
17626-86-7
反应条件
tert.-butylhydroperoxide; ferric acetate; trifluoroacetic acid in acetic acid 4 h; Heating;
参考文献
Fontana, Francesca; Minisci, Francesco; Barbosa, Maria Claudia Nogueira; Vismara, Elena
Acta Chemica Scandinavica, 1989 , vol. 43, # 10 p. 995 - 999
95-16-9
苯并噻唑
+
75-98-9
→
反应条件
17626-88-9
反应条件
dipotassium peroxodisulfate; silver nitrate in dichloromethane; water T=20°C; 8 h; Reagent/catalystSolvent;
参考文献
Zhao, Wei-Ming; Chen, Xiao-Lan; Yuan, Jin-Wei; Qu, Ling-Bo; Duan, Li-Kun; Zhao, Yu-Fen
Chemical Communications, 2014 , vol. 50, # 16 p. 2018 - 2020
95-16-9
苯并噻唑
+
38442-51-2
→
反应条件
35844-59-8
+
17626-88-9
反应条件
potassium iodide in dimethyl sulfoxide T=35 - 40°C; Irradiation;
参考文献
Russell, Glen A.; Wang, Lijuan; Rajaratnam, Ragine
Journal of Organic Chemistry, 1996 , vol. 61, # 25 p. 8988 - 8991
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