4-氯-1,2-苯二胺合成路线 （共 167 条）
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane 4 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
反应条件
tin(ll) chloride in methanol; water Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 76, # 1 p. 76 - 81
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate 2: palladium on activated charcoal; ammonium formate / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 17 p. 4790 - 4793
参考文献
Helvetica Chimica Acta, , vol. 11, p. 780
反应条件
1: acetic acid 2: aq. NaOH View Scheme
参考文献
Zhang, Lei; Chen, Xiaojie; Liu, Jun; Zhu, Qingzhang; Leng, Ying; Luo, Xiaomin; Jiang, Hualiang; Liu, Hong
European Journal of Medicinal Chemistry, 2012 , vol. 58, p. 624 - 639
反应条件
in diethylene glycol dimethyl ether T=140°C; 24 h;
参考文献
Climent; Corma; Hernandez; Hungria; Iborra; Martinez-Silvestre
Journal of Catalysis, 2012 , vol. 292, p. 118 - 129
反应条件
sodium acetate in acetic acid T=60°C; 2 h;
参考文献
Okafor
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 1 p. 149 - 153
反应条件
in water T=20°C; 0.5 h; Green chemistry;
参考文献
Delpivo, Camilla; Micheletti, Gabriele; Boga, Carla
Synthesis (Germany), 2013 , vol. 45, # 11 art. no. SS-2013-Z0031-OP, p. 1546 - 1552
反应条件
in ethanol; water 3 h; Heating;
参考文献
Rtishchev; Selitrennikov
Russian Journal of General Chemistry, 2004 , vol. 74, # 3 p. 428 - 437
反应条件
acetic acid T=20°C; 1.16667 h; Cooling;
参考文献
Zhang, Lei; Chen, Xiaojie; Liu, Jun; Zhu, Qingzhang; Leng, Ying; Luo, Xiaomin; Jiang, Hualiang; Liu, Hong
European Journal of Medicinal Chemistry, 2012 , vol. 58, p. 624 - 639
