1,2,4,5-四甲基苯合成路线 (共 381 条)
参考文献
Smith; Rosenbaum
Journal of the American Chemical Society, 1951 , vol. 73, p. 3843,3846
反应条件
nitrous acid methyl ester; nitrogen(II) oxide T=24.84°C; P=735 Torr; Irradiation; Kinetics;
参考文献
Aschmann, Sara M.; Arey, Janet; Atkinson, Roger
Journal of Physical Chemistry A, 2013 , vol. 117, # 12 p. 2556 - 2568
反应条件
in acetonitrile T=10°C; 24 h; IrradiationΔG investigated; Thermodynamic dataProduct distribution;
参考文献
Koshima, Hideko; Chisaka, Yosuke; Wang, Yang; Yao, Xinkan; Wang, Honggen; et al.
Tetrahedron, 1994 , vol. 50, # 48 p. 13617 - 13630
参考文献
Nippon Steel Chemical Co., Ltd.
Patent: US6369240 B1, 2002 ;
Location in patent: Page column 12 ;
反应条件
dinitrogen tetraoxide in various solvent(s) T=-78°C; 48 h; Irradiation; Further byproducts given;
参考文献
Bosch, E.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3314 - 3325
反应条件
3,4,5,6-tetrachloro-1,2-benzoquinone T=140°C; 24 h;
参考文献
Kobayashi, Tomoshige; Rahman, Sheikh Maksudur
Synthetic Communications, 2003 , vol. 33, # 22 p. 3997 - 4003
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 1.5 h; Further byproducts given;
参考文献
Bosch, E.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3314 - 3325
反应条件
lithium trifluoroacetate in trifluoroacetic acid Kinetics; solns. of Tl(OCOCF3)3, arene, and CF3COOLi in degassed CF3COOH were mixed at 25°C under Ar in the dark, mixt. was stirred for 1-3 h; rate const. is given; reaction was quenched with aq. KI, extd. with CH2Cl2, resulting aryl iodide and other products were sepd. and identified by gas chromy. and mass spectrum (iodide, dimer);
参考文献
Lau, W.; Kochi, J. K.
Journal of the American Chemical Society, 1984 , vol. 106, # 23 p. 7100 - 7112
反应条件
2,6-di-tert-butyl-4-methylpyridine; oxygen; NOBF4 in dichloromethane T=3°C; 24 h;
参考文献
Kim, E. K.; Kochi, J. K.
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1692 - 1702
反应条件
NOBF4 in acetonitrile T=25°C; 5.5 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bosch, Eric; Kochi, Jay K.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5573 - 5586