1,2,4,5-四甲基苯合成路线 (共 381 条)
反应条件
sulfuric acid in water; acetic acid T=90°C; 3 h; Product distributionMechanism;
参考文献
Gorodetskaya, T. A.; Kozhevnikov, I. V.; Matveev, K. I.; Sidel'nikov, V. N.; Maksimovskaya, R. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 929 - 935
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1010 - 1017
反应条件
nitrosyl chloride; trifluoroacetic acid T=20°C; 4.5 h; other time; Product distributionMechanism;
参考文献
Makhon'kov, D. I.; Cheprakov, A. V.; Rodkin, M. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 2 p. 211 - 217
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 2 p. 241 - 248
反应条件
1: (i) NBS, (PhCO)2O2, CCl4, (ii) /BRN= 956566/, Et2O 2: (i) Ag2O, (ii) phenothiazine, toluene View Scheme
参考文献
Longone,D.T.; Chow,H.S.
Journal of the American Chemical Society, 1970 , vol. 92, p. 994 - 998
反应条件
hydrogenchloride; potassium permanganate in water 0.0833333 h; Photolysis;
参考文献
Zenkevich
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 2 p. 270 - 280
反应条件
1.1: bromine / tetrachloromethane / 54 °C / Darkness 1.2: Irradiation; Reflux 2.1: sodium o-vanadate; nitric acid / Reflux 3.1: 205 °C View Scheme
参考文献
Guo, Xugang; Watson, Mark D.
Macromolecules, 2011 , vol. 44, # 17 p. 6711 - 6716
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Bosch, E.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3314 - 3325
反应条件
sodium iodide in acetonitrile
参考文献
Okazaki, Takao; Laali, Kenneth K.; Bunge, Scott D.; Adas, Sonya K.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 8 p. 1630 - 1644
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Bosch, E.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3314 - 3325
反应条件
triethylamine in 2,2,2-trifluoroethanol 7 h; Photolysis;
参考文献
Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6495 - 6498
反应条件
in 1,1,2,2-tetrachloroethylene 24 h; Heating;
参考文献
Molecules, , vol. 7, # 11 p. 840 - 847