3,6-二甲基-1,4-二氧杂环己烷-2,5-二酮合成路线 （共 32 条）
反应条件
1: With potassium hydroxide T=105 - 115°C; pH=11; 4 h; 2: With 2-hydroxypropionic acid pH=~ 8; 3: T=135°C; 4 h; Reflux; Product distribution / selectivity;
参考文献
GALACTIC S.A.
Patent: US2012/203032 A1, 2012 ;
Location in patent: Page/Page column 3 ;
反应条件
amberlyst wet 15 T=130°C;
参考文献
Van Wouwe, Pieter; Dusselier, Michiel; Basic, Aurelie; Sels, Bert F.
Green Chemistry, 2013 , vol. 15, # 10 p. 2817 - 2824
参考文献
Wurtz; Friedel
Annales de Chimie (Cachan, France), 1861 , vol. <3> 63, p. 108
Full Text Show Details
Pelouze
Justus Liebigs Annalen der Chemie, 1845 , vol. 53, p. 116
反应条件
amberlyst wet 15 T=130°C;
参考文献
Van Wouwe, Pieter; Dusselier, Michiel; Basic, Aurelie; Sels, Bert F.
Green Chemistry, 2013 , vol. 15, # 10 p. 2817 - 2824
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=35°C; 5 h;
参考文献
Nederberg; Connor; Glausser; Hedrick
Chemical Communications, 2001 , # 20 p. 2066 - 2067
参考文献
Craciun, Liliana; Benn, Gerald P.; Dewing, John; Schriver, George W.; Peer, William J.; Siebenhaar, Bernd; Siegrist, Urs
Patent: US2005/222458 A1, 2005 ;
Location in patent: Page/Page column 10 ;
反应条件
[EtZn(η(3)-C6H6)][CHB11Cl11]*C6H6 in benzene-d6
T=90°C; 23 h;
参考文献
Wehmschulte, Rudolf J.; Wojtas, Lukasz
Inorganic Chemistry, 2011 , vol. 50, # 22 p. 11300 - 11302
参考文献
Bischoff; Walden
Chemische Berichte, vol. 279, p. 73
反应条件
(10H)-phenothiazine; nickel diacetate; nickel(II) nitrate hexahydrate
T=225°C; P=26618.1 Torr; 4 h; Autoclave;
参考文献
Fruchey, Olan S.; Maliszewski, Thomas A.; Sawyer, John E.
Patent: US2012/78004 A1, 2012 ;
Location in patent: Page/Page column 3 ;
参考文献
SYNGENTA LIMITED
Patent: US2009/227453 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
