D-alpha,beta-环己亚基甘油合成路线 （共 6 条）
反应条件
oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-60°C; Swern oxidation;
参考文献
Bianchi, Paola; Roda, Gabriella; Riva, Sergio; Danieli, Bruno; Zabelinskaja-Mackova, Antonina; Griengl, Herfried
Tetrahedron, 2001 , vol. 57, # 11 p. 2213 - 2220
反应条件
pig liver esterase; vinyl propionate; water; methoxypolyethylene glycol in toluene T=20°C; kinetic resolution; 408 h; Title compound not separated from byproducts;
参考文献
Jungen, Manfred; Gais, Hans-Joachim
Tetrahedron Asymmetry, 1999 , vol. 10, # 19 p. 3747 - 3758
反应条件
4 A molecular sieve; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-2-[(N-benzyl-N-methylamino)methyl]pyrrolidine in dichloromethane; N,N-dimethyl-formamide T=-78°C; 3 h; Title compound not separated from byproducts;
参考文献
Terakado, Dai; Koutaka, Hitomi; Oriyama, Takeshi
Tetrahedron Asymmetry, 2005 , vol. 16, # 6 p. 1157 - 1165
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: indium trifluoromethanesulfonate / dichloromethane / 20 °C<br />2: indium trifluoromethanesulfonate / 0.5 h / 20 °C / Neat (no solvent)<br /> <br />
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E. Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '23479886', constants.ctx, '0')">graphene</a> <br />T=100°C; 2 h; Sealed tubeGreen chemistry; Catalytic behavior; <br />
参考文献
Oger, Nicolas; Lin, Yuting F.; Le Grognec, Erwan; Rataboul, Franck; Felpin, Franois-Xavier Green Chemistry, 2016 , vol. 18, # 6 p. 1531 - 1537
反应条件
<b>With</b> amberlyst 15<br />T=56°C; 0.333333 h; <br />
参考文献
Vol'Eva; Belostotskaya; Malkova; Komissarova; Kurkovskaya; Usachev; Makarov Russian Journal of Organic Chemistry, 2012 , vol. 48, # 5 p. 638 - 641
