2,4,6-三甲基苯甲酮合成路线 (共 76 条)
反应条件
LDPA in tetrahydrofuran T=61°C; 14 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 5907 - 5914
反应条件
lithium dimesityl borohydride bis(dimethoxyethane); 2,2'-azo-bisisobutyronitrile in N,N-dimethyl-formamide T=61°C;
参考文献
Tanner, Dennis D.; Xie, Guo-Jian; Hooz, John; Yang, Chi-Ming
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7138 - 7142
反应条件
1: AlCl3 / CS2 2: lithium dimesityl borohydride bis(dimethoxyethane) / AIBN / dimethylformamide / 61 °C / other solvent and temperature; also in a presence of DNB View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7138 - 7142
反应条件
in tetrahydrofuran T=-15 - 20°C; 3 h;
参考文献
Lee, Jae In
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 3 p. 749 - 752
反应条件
bis-triphenylphosphine-palladium(II) chloride in toluene T=90°C; Stille Cross Coupling; 0.5 h; Inert atmosphere;
参考文献
Luong, Martin; Domini, Claudia E.; Silbestri, Gustavo F.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2013 , vol. 723, p. 43 - 48
反应条件
trifluoroacetic acid 10 h; Heating;
参考文献
Keumi, Takashi; Taniguchi, Rikio; Kitajima, Hidehiko
Synthesis, 1980 , # 2 p. 139 - 141
反应条件
trifluorormethanesulfonic acid in nitromethane T=100°C; 6 h; Yield given;
参考文献
El-Khagawa, Ahmed M.
Bulletin de la Societe Chimique de France, 1987 , # 2 p. 372 - 374
参考文献
Gu, Taiyin Yang; Weber, William P.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2541 - 2544
反应条件
trifluoroacetic acid 5 h; Heating;
参考文献
Keumi, Takashi; Saga, Hiroshi; Kitajima, Hidehiko
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1638 - 1641
参考文献
Effenberger, Franz; Sohn, Erich; Epple, Gerhard
Chemische Berichte, 1983 , vol. 116, # 3 p. 1195 - 1208