反应条件
Na in ammonia
NH3 (liquid); To a suspn. of Ph2BiI in liquid NH3 sodium sand was added for about 30 min, temp. between -80 and -50°C, inert atm.;; ppt. was filtered, extd. with toluene at room temp., soln. was filtered, evapd., to dryness, recrystd. from hot abs. EtOH; elem. anal.;;
参考文献
Calderazzo, Fausto; Poli, Rinaldo; Pelizzi, Giancarlo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 2365 - 2370