反应条件
1: 1.) NaH / 1.) reflux, 3 h, 2.) a) RT, 30 min, b) reflux, 4 h
2: 93 percent / pyridinium chlorochromate / CH2Cl2 / 12 h
3: 99 percent / triethylamine / dimethylformamide / Heating
4: 1.) H2O, p-toluenesulfonic acid, 2.) periodic acid / 1.) CH3OH, reflux, 1 h, 2.) CH3OH, RT, 2 h
View Scheme
参考文献
Kachinski,J.L.C.; Salomon,R.G.
Tetrahedron Letters, 1977 , p. 3235 - 3238
