1,3-二氯-2-丙醇合成路线 (共 217 条)
参考文献
Annales de Chimie (Cachan, France), , vol. <6> 22, p. 482
Justus Liebigs Annalen der Chemie, , vol. 159, p. 176
Chemische Berichte, , vol. 21, p. 1285
Chemische Berichte, , vol. 24, p. 2670
反应条件
potassium carbonate; Co(II)(3,5-Cl,Cl-sal)2(S-CHXDA) (e.e. 1.) 130-150 deg C, 3 hr in vacuo; 2.) CH2Cl2, 25 deg C, 6 days; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Li, Wenji; Thakur, Santosh Singh; Chen, Shu-Wei; Shin, Chang-Kyo; Kawthekar, Rahul B.; Kim, Geon-Joong
Tetrahedron Letters, 2006 , vol. 47, # 20 p. 3453 - 3457
反应条件
in benzyl alcohol Etherification; 1.5 h; Heating;
参考文献
Doyle, Michael P.; Tedrow, Jason S.; Dyatkin, Alexey B.; Spaans, Coenraad J.; Ene, Doina G.
Journal of Organic Chemistry, 1999 , vol. 64, # 24 p. 8907 - 8915
反应条件
sodium hydride T=100°C;
参考文献
Ogilvie; Nguyen-Ba; Gillen; et al.
Canadian Journal of Chemistry, 1984 , vol. 62, # 2 p. 241 - 252
反应条件
sodium hydroxide; benzyl alcohol T=140 - 150°C;
参考文献
Tsatsas
Annales Pharmaceutiques Francaises, 1950 , vol. 8, p. 273,285
反应条件
ethanol T=115 - 120°C;
参考文献
Gorini
Gazzetta Chimica Italiana, 1933 , vol. 63, p. 753
反应条件
potassium carbonate in N,N-dimethyl-formamide T=135°C; 8 h;
参考文献
Farhanullah; Ji Ram, Vishnu
Synlett, 2009 , # 14 p. 2265 - 2268
参考文献
Fairbourne; Gibson; Stephens
Journal of the Chemical Society, 1932 , p. 1966,1968
Full Text Show Details
Stephens
Chemistry and Industry (London, United Kingdom), 1932 , p. 375,377
参考文献
Levas
Annales de Chimie (Cachan, France), 1948 , vol. <12> 3, p. 145,191
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 223, p. 901,903 Anm.
参考文献
Roessing
Chemische Berichte, 1886 , vol. 19, p. 64