sulfuric acid T=125°C; 5 h; other temperatures, other reaction times; Product distribution;

sodium hydroxide in ice-water; water

暂无反应条件数据

thionyl chloride in N,N-dimethyl-formamide 4 h; Reflux;

sodium hydroxide in water T=20°C; 1 h;

1.1: N,N-dimethyl-formamide; thionyl chloride / 4 h / Reflux 2.1: ammonium hydroxide / toluene; water; tetrahydrofuran / 2 h / -10 °C / Reflux 2.2: pH 4 3.1: ammonium hydroxide; (NH4)2CO3; copper(II) sulfate / water / 72 h / 118 °C / Autoclave; Industry scale 4.1: hydrogen / palladium 10 on activated carbon / tetrahydrofuran; methanol / 23 °C / 2585.81 Torr / Industry scale; Autoclave View Scheme

暂无反应条件数据

1: With thionyl chloride in N,N-dimethyl-formamide Heating / reflux; 2: With ammonia in tetrahydrofuran; water; N,N-dimethyl-formamide; toluene T=-10°C; 2 h; 3: With hydrogenchloride in tetrahydrofuran; water; N,N-dimethyl-formamide; toluene pH=4; Product distribution / selectivity;

ammonia T=150°C; unter Druck;

barium dihydroxide; iron(II) sulfate