(R)-2- [N-(N-苄基脯氨酰）氨基]二苯甲酮合成路线 （共 15 条）
反应条件
nickel nitrate; water; sodium methylate; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259
反应条件
nickel nitrate; water; sodium methylate; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259
反应条件
nickel nitrate; water; sodium methylate; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259
反应条件
nickel nitrate; water; triethyl amine hydrochloride; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259
反应条件
nickel nitrate; water; triethyl amine hydrochloride; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259
反应条件
sodium methoxide in methanol a soln. of glycine in MeONa-MeOH was added to a soln. of the substituted benzophenone and Ni(NO3)2*6H2O in MeOH, mixt. was stirred for 2 h at 50°C under Ar, reaction was monitored by TLC; water was added, mixt. extd. with CHCl3, ext. evapd., residue purified on SiO2 and Sephadex LH-20 columns (eluents CHCl3-acetone and benzene-EtOH resp.); elem. anal.;
参考文献
Belokon, Yuri N.; Bulychev, Alexander G.; Vitt, Sergei V.; Struchkov, Yuri T.; Batsanov, Andrei S.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4252 - 4259
反应条件
sodium tetrahydroborate; triethylamine; nickel(II) nitrate hexahydrate Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belokon, Yuri N.; Bulychev, Aleksandr G.; Ryzhov, Mikhail G.; Vitt, Sergei V.; Batsanov, Andrei S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1865 - 1872
反应条件
hydrogenchloride; Ni(CO)32; sodium methylate Multistep reaction;
参考文献
Belokon', Yu. N.; Tararov, V. I.; Savel'eva, T. F.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 5.2 p. 1054 - 1058
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 5 p. 1175 - 1180
反应条件
nickel nitrate; water; sodium methylate; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 107, # 14 p. 4252 - 4259
反应条件
nickel nitrate; water; sodium methylate; triethylamine 1.) MeOH, 2 h, 50 deg C; 2.) MeOH, 50 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 107, # 14 p. 4252 - 4259
