1-氯-2,4-二硝基苯合成路线 (共 755 条)
参考文献
Journal of the Chemical Society, , p. 720
Journal of the Chemical Society, , p. 18
反应条件
39 h; Heating; Product distribution;
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 3072 - 3083
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 78, p. 261
参考文献
Bordwell; Hewett
Journal of Organic Chemistry, 1957 , vol. 22, p. 980
反应条件
1: ethyl acetate / 1 h / Heating 2: 63 percent / sodium sulphide, sulphur / ethanol; H2O / 0.5 h / Heating 3: 93 percent / copper(II) acetate / dimethylformamide / 0.5 h / 100 °C 4: 89 percent / pyridine / 0.5 h / Heating 5: 88 percent / various solvent(s) / 1.5 h / 100 °C 6: 52 percent / POCl3 / 1 h / Heating 7: 49 percent / various solvent(s) / 1.25 h / 80 °C View Scheme
参考文献
Chambers, David; Denny, William A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1055 - 1060
反应条件
copper T=200°C; 1.5 h;
参考文献
Bell, Anthony J.; Read, Roger W.
Australian Journal of Chemistry, 1987 , vol. 40, # 11 p. 1813 - 1829
反应条件
ethanol; sodium hydrogencarbonate
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 65, p. 321
反应条件
sodium hydroxide; potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in benzene 15 h; Heating;
参考文献
Moreno-Manas, M.; Sanchez-Ferrando, F.; Valle, S.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1577 - 1579
反应条件
1: ethyl acetate / 1 h / Heating 2: 63 percent / sodium sulphide, sulphur / ethanol; H2O / 0.5 h / Heating 3: 93 percent / copper(II) acetate / dimethylformamide / 0.5 h / 100 °C 4: 89 percent / pyridine / 0.5 h / Heating 5: 88 percent / various solvent(s) / 1.5 h / 100 °C 6: 52 percent / POCl3 / 1 h / Heating 7: 49 percent / various solvent(s) / 1.25 h / 80 °C 8: 85 percent / KOH / methanol / 0.5 h / Heating View Scheme
参考文献
Chambers, David; Denny, William A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1055 - 1060