1-氯-2,4-二硝基苯合成路线 (共 755 条)
参考文献
Tin-Lok,C. et al.
Journal of the Chemical Society, 1964 , p. 1213 - 1216
参考文献
Biffin,M.E.C.; Paul,D.B.
Australian Journal of Chemistry, 1974 , vol. 27, p. 777 - 788
反应条件
potassium hydroxide; Aliquat
T=20°C; 0.5 h; other halogenonitrobenzenes and halogenobenzenes and other arylhalides; other tetraalkylammonium salt , other solid bases; other nucleophiles; var. temp. and time; Product distribution;
参考文献
Loupy, Andre; Philippon, Noelle; Pigeon, Philippe; Sansoulet, Jean; Galons, Herve
Synthetic Communications, 1990 , vol. 20, # 18 p. 2855 - 2864
参考文献
The Dow Chemical Company
Patent: US4642349 A1, 1987 ;
反应条件
octane; water; lt;2-n-tridecyl(1,3-dioxolan-4-yl)methylgt;trimethylammonium bromide; butan-1-ol
T=50°C; 0.5 h;
参考文献
Bieniecki, A.; Matuszewska, B.; Wilk, K. A.
Polish Journal of Chemistry, 1995 , vol. 69, # 8 p. 1174 - 1181
参考文献
Willgerodt
Chemische Berichte, 1879 , vol. 12, p. 763
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Maikopar
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1873 , vol. 5, p. 46
Chemische Berichte, 1873 , vol. 6, p. 564
反应条件
in methanol
T=25 - 45°C; Ea, ΔH; Rate constantThermodynamic dataKinetics;
参考文献
Kharaba, Mohamed A. H.; Nassar, Ahmad M. G.; Youssef, Abdel-Hamid A.; Faid-Allah, Hassan M.
Polish Journal of Chemistry, 1991 , vol. 65, # 5-6 p. 1029 - 1034
反应条件
T=40°C; further temperatures, E(activ.), ΔG(activ.), ΔH(activ.), ΔS(activ.); KineticsMechanismThermodynamic data;
参考文献
El-Kholy, Ali E.; Kasem, Taher S.; El-Kashlan, Howaida M.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1989 , vol. 28, # 5 p. 388 - 391
反应条件
2,4-diamino-toluene; potassium carbonate; copper(I) bromide in 1-methyl-pyrrolidin-2-one
T=110°C; Goldberg reaction; 1 h; Inert atmosphere;
参考文献
Chen, Zheng; Wu, Yiran; Liu, Ying; Yang, Suijia; Chen, Yunjie; Lai, Luhua
Journal of Medicinal Chemistry, 2011 , vol. 54, # 10 p. 3650 - 3660
反应条件
copper
T=150 - 160°C;
参考文献
Brewster; Choguill
Journal of the American Chemical Society, 1939 , vol. 61, p. 2702