N-乙酰基-DL-丝氨酸合成路线 （共 11 条）
反应条件
pyridine in water Ambient temperature;
参考文献
Rose, Janet E.; Leeson, Paul D.; Gani, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 21 p. 3089 - 3094
反应条件
water; lithium hydroxide hydrate in methanol 0.5 h;
参考文献
Organic Letters, , vol. 13, # 20 p. 5652 - 5655
参考文献
Journal of the American Chemical Society, , vol. 81, p. 1751,1752
参考文献
Biochimica et Biophysica Acta, , vol. 30, p. 352,354
反应条件
hydrogenchloride; methyloxirane 1) reflux, 2 h; 2) ethanol, reflux, 15 min; Yield given. Multistep reaction;
参考文献
Rose, Janet E.; Leeson, Paul D.; Gani, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 21 p. 3089 - 3094
反应条件
potassium hydroxide; potassium phosphate buffer; porcine kidney acylase I T=40°C; relative initial rate of hydrolysis, also with Aspergillus acylase I as a catalyst; with or without CoCl2;
参考文献
Journal of the American Chemical Society, , vol. 111, # 16 p. 6354 - 6364
反应条件
potassium hydroxide; potassium phosphate buffer; porcine kidney acylase I T=40°C; relative initial rate of hydrolysis, also with Aspergillus acylase I as a catalyst; with or without CoCl2;
参考文献
Ngamsom; Hickey; Greenway; Littlechild; Watts; Wiles
Journal of Molecular Catalysis B: Enzymatic, 2010 , vol. 63, # 1-2 p. 81 - 86
反应条件
1: 69 percent / conc. H2SO4 / 6 h / Heating
2: 78 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, CuCl / acetonitrile / 24 h / 40 °C
View Scheme
参考文献
Bell, Natalie V.; Bowman, W. Russell; Coe, Paul F.; Turner, Andrew T.; Whybrow, Del
Canadian Journal of Chemistry, 1997 , vol. 75, # 6 p. 873 - 883
反应条件
N,N'-disuccinimidyl-carbonate; triethylamine
1.) CH3CN, RT, 3 h, 2.) RT, 1 h; Yield given. Multistep reaction;
参考文献
Mayoral, J. A.; Cativiela, C.; Lopez, M. P.; Ojo, D.; Zuane, F. De
Journal of Crystallographic and Spectroscopic Research, 1989 , vol. 19, # 6 p. 993 - 1002
反应条件
acetic anhydride; acetic acid
T=80°C; 1.5 h; Inert atmosphere;
参考文献
Yokoyama, Yuusaku; Nakakoshi, Masamichi; Okuno, Hiroaki; Sakamoto, Yohko; Sakurai, Satoshi
Magnetic Resonance in Chemistry, 2010 , vol. 48, # 10 p. 811 - 817
