甲基α-D-吡喃葡萄糖苷合成路线 (共 276 条)
反应条件
pyridine in N,N-dimethyl-formamide 72 h; Ambient temperature; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 202, p. 67 - 79
反应条件
bis(tri-n-butyltin)oxide 1) toluene, reflux, 4 h, 2) r.t., 18 h; Yield given. Multistep reaction;
参考文献
Koch; Chambers
Carbohydrate Research, 1993 , vol. 241, p. 295 - 299
参考文献
Bourne et al.
Journal of the Chemical Society, 1949 , p. 2976,2978
反应条件
pyridine; 1,1,1,3,3,3-hexachloro-propan-2-one 1.) DMF, r.t., 3 d; 2.) 12 h; Multistep reaction. Yields of byproduct given;
参考文献
Haines, Alan H.; Sutcliffe, E. John
Carbohydrate Research, 1985 , vol. 138, p. 143 - 147
反应条件
pyridine 1.) DMF, r.t., 3 d; 2.) 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Haines, Alan H.; Sutcliffe, E. John
Carbohydrate Research, 1985 , vol. 138, p. 143 - 147
反应条件
pyridine; zinc(II) chloride in N,N-dimethyl-formamide 72 h; Ambient temperatureor -15 deg C; effect of additives; analogous reactions with methyl β-D-glucopyranoside (ZnCl2) and further methyl α-D-hexopyranosides; Product distribution;
参考文献
Hanessian, Stephen; Kagotani, Masahiro
Carbohydrate Research, 1990 , vol. 202, p. 67 - 79
反应条件
1: pyridine / 48 h / 20 °C / |Glovebox 2: [(2,6-[OP(tBu)2]2C6H3)Ir(H)(acetone)]+[B(C6F5)4]-; diethylesilane / 336 h / |Inert atmosphere; |Glovebox View Scheme
参考文献
McLaughlin, Matthew P.; Adduci, Laura L.; Becker, Jennifer J.; Gagne, Michel R.
Journal of the American Chemical Society, 2013 , vol. 135, # 4 p. 1225 - 1227
反应条件
hydrogenchloride in water T=85°C; Inert atmosphere; Kinetics; SolventReagent/catalyst;
参考文献
Phan, Hung Duy; Yokoyama, Tomoya; Matsumoto, Yuji
Journal of Carbohydrate Chemistry, 2013 , vol. 32, # 4 p. 223 - 239
反应条件
sulfuric acid; acetic acid in water 6 h; Reflux;
参考文献
Li, Tiehai; Guo, Lina; Zhang, Yan; Wang, Jiajia; Zhang, Zhenxing; Li, Jing; Zhang, Wenpeng; Lin, Jianping; Zhao, Wei; Wang, Peng George
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2136 - 2144
反应条件
Bacillus macerans cyclomaltodextrin glucanyltransferase in acidic aq. solution T=37°C; pH=6.0; 24 h; Further byproducts given;
参考文献
Yoon, Seung-Heon; Robyt, John F.
Carbohydrate Research, 2006 , vol. 341, # 2 p. 210 - 217