反应条件
in toluene
metal and S-compd. were refluxed in 1:1.5 molar ratio in toluene for 3 h; soln. was filtered, concd. to 1/3 of its original vol., cooled to room temp., solid was filtered off, washed with petroleum ether (b.p. 60-80 °C), dried in vac., elem. anal.;
参考文献
Mustafa; Taqa, Amer A.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 2001 , vol. 31, # 4 p. 517 - 526
