反应条件
in diethyl ether; toluene K. Ziegler and W. P. Neumann, DBP 1 157 617 (1959/63); to stirred soln.of AlEt3 in toluene dropwise added SnCl4 and then Et2O at -25 °C, warmed to room temp., heated for 2 h at 80 °; cooled to -50 °C, added HCl, org. layer washed with Et2O, dried over Na2SO4, distd. in vac.;
参考文献
Journal of Organometallic Chemistry, , vol. 234, # 3 p. 277 - 286