1: 1-benzyltetrahydro-1H-thiophenium triflate With lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 0.333333 h; 2: triethyl borane With triphenylborane in tetrahydrofuran T=-105 - 20°C; 3: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=0 - 20°C;
参考文献
Howells, Dean; Robiette, Raphael; Fang, Guang Y.; Knowles, Luke S.; Woodrow, Michael D.; Harvey, Jeremy N.; Aggarwal, Varinder K.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 7 p. 1185 - 1189
1: triethyl borane With magnesium in tetrahydrofuran; N,N-dimethyl acetamide T=27°C; 2: 5-tetrakis (dibromomethyl)-benzene in tetrahydrofuran; N,N-dimethyl acetamide T=27°C; 3: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; N,N-dimethyl acetamide; water
参考文献
Condon, Sylvie; Nedelec, Jean-Yves
Journal of Organometallic Chemistry, 2010 , vol. 695, # 1 p. 32 - 35
