mixing of B(C2H5)3 and (C4H9)2O*BF3 at room temp., addn. of ethyldiborane(6) and heating to 100°C; first C2H5BF2 distilled, then (C2H5)2BF;
参考文献
Koester, R.; Grassberger, M. A.
Liebigs Annalen der Chemie, 1968 , vol. 719, p. 169 - 186
Full Text Show Details
Gmelin Handbook: B: B-Verb.9, 6.1, page 258 - 268
Koester, R.; Grassberger, M. A.
Liebigs Annalen der Chemie, 1968 , vol. 719, p. 169 - 186
Full Text Show Details
Gmelin Handbook: B: B-Verb.9, 6.1, page 258 - 268
Laurent, J. P.; Tuchagues, J. P.; Gallais, F.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1968 , vol. 267, p. 789 - 792
Full Text Show Details
Gmelin Handbook: B: B-Verb.9, 6.1, page 258 - 268
1: With tri-tert-butyl phosphine; sodium carbonate; bis(1,5-cyclooctadiene)nickel (0) in diethyl ether; water
T=20°C; 6 h;
2: With hydrogenchloride
Further stages.;