chloro-trimethyl-silane; zinc in tetrahydrofuran
T=50°C; 3 h; Yield givenYields of byproduct given;
参考文献
Ishino, Yoshio; Mihara, Masatoshi; Nishihama, Shintaro; Nishiguchi, Ikuzou
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 11 p. 2669 - 2672
Lippmann; Luginin
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1867 , vol. 65, p. 349
Justus Liebigs Annalen der Chemie, 1868 , vol. 145, p. 107
in ethanol
byproducts: HCl; Irradiation (UV/VIS); radiation of a Hg high pressure lamp; also formation of decompn. products of ferrocene;;
参考文献
Akiyama, T.; Hoshi, Y.; Gogo, S.; Sugimori, A.
Bulletin of the Chemical Society of Japan, 1973 , vol. 46, p. 1851 - 1854
Full Text Show Details
Gmelin Handbook: Fe: Org.Verb.A1, 2.5.8.8, page 187 - 190
hydrogenchloride in chloroform-d1
T=190°C; 15 h; Title compound not separated from byproducts;
参考文献
De'ath, Norman J.; Miller, Allen J.; Nunn, John M.; Stewart, Denis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 776 - 784
