叔丁基 2,2,2-三氯乙酰亚胺酯合成路线 （共 44 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane 16 h; Ambient temperature;
参考文献
Armstrong, Alan; Brackenridge, Ian; Jackson, Richard F.W.; Kirk, Joanna M.
Tetrahedron Letters, 1988 , vol. 29, # 20 p. 2483 - 2486
反应条件
1: in dichloromethane; cyclohexane 4.5 h; 2: With boron trifluoride diethyl etherate in cyclohexane; water-d2 3: With water; sodium hydrogencarbonate in dichloromethane; cyclohexane 1 h;
参考文献
WO2007/106546 A2, ;
Page/Page column 12-13 ;
反应条件
boron trifluoride-diethyl ether complex in dichloromethane; cyclohexane
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane 16 h; Ambient temperature;
参考文献
Armstrong, Alan; Brackenridge, Ian; Jackson, Richard F.W.; Kirk, Joanna M.
Tetrahedron Letters, 1988 , vol. 29, # 20 p. 2483 - 2486
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane T=20°C; 16 h;
参考文献
Kang, Sang-Uk; Shi, Zhen-Dan; Worthy, Karen M.; Bindu, Lakshman K.; Dharmawardana, Pathirage G.; Choyke, Sarah J.; Bottaro, Donald P.; Fisher, Robert J.; Burke Jr., Terrence R.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 12 p. 3945 - 3948
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane; cyclohexane T=0 - 20°C; 0.75 h; 2: With sodium hydrogencarbonate in dichloromethane; cyclohexane
参考文献
CHROMA THERAPEUTICS LTD.
Patent: WO2008/50096 A1, 2008 ;
Location in patent: Page/Page column 48-49 ;
WO 2008/050096 A1
反应条件
sodium hydrogencarbonate; boron trifluoride-diethyl ether complex in tetrahydrofuran; dichloromethane; cyclohexane
反应条件
boron trifluoride diethyl etherate in pentane 1.) -5 deg C, 15 min, 2.) up to r.t.;
参考文献
Tetrahedron, , vol. 49, # 12 p. 2477 - 2484
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Claeys, Magda; Szmigielski, Rafal; Kourtchev, Ivan; Van Der Veken, Pieter; Vermeylen, Reinhilde; Maenhaut, Willy; Jaoui, Mohammed; Kleindienst, Tadeusz E.; Lewandowski, Michael; Offenberg, John H.; Edney, Edward O.
Environmental Science and Technology, 2007 , vol. 41, # 5 p. 1628 - 1634
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran T=20°C;
参考文献
Lorthioir; McKeown; Parr; Washington; Watson
Tetrahedron Letters, 2000 , vol. 41, # 44 p. 8609 - 8613
