3.5-二硝基苯甲酰氯合成路线 (共 144 条)
参考文献
Boese; Jones; Major
Journal of the American Chemical Society, 1931 , vol. 53, p. 3530,3534
反应条件
calcium hydroxide powder in 1,4-dioxane
0.5 h; Heating;
参考文献
Arora, H. C.; Rao, G. N.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1981 , vol. 20, # 5 p. 539 - 540
反应条件
1: aq. NaOH solution; benzene
2: NaI; acetone
View Scheme
参考文献
Heine et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2202
反应条件
triethylamine in dichloromethane
T=20°C; 2 h; Inert atmosphere;
参考文献
Iwaniuk, Daniel P.; Wolf, Christian
Journal of Organic Chemistry, 2010 , vol. 75, # 19 p. 6724 - 6727
参考文献
Deshmukh, M.; Dunnach, E.; Juge, S.; Kagan, H. B.
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3467 - 3470
反应条件
N-ethyl-N,N-diisopropylamine
参考文献
Czerwenka, Christoph; Zhang, Mei Mei; Kaehlig, Hanspeter; Maier, Norbert M.; Lipkowitz, Kenny B.; Lindner, Wolfgang
Journal of Organic Chemistry, 2003 , vol. 68, # 22 p. 8315 - 8327
参考文献
Vogel,A.I.
Text-Book of Practical Organic Chemistry, 1. Aufl. <London 1948> S. 263, 268, 3. Aufl. <London 1956> S. 262, 268
反应条件
triethylamine in tetrahydrofuran
T=20°C; 20 h;
参考文献
Tokai University
Patent: EP1528063 A1, 2005 ;
Location in patent: Page/Page column 16 ;
反应条件
in pyridine; acetone
10 h; Ambient temperature;
参考文献
Bayer, Ernst; De-Qing, Wei; Geckeler, Kurt
Chemische Berichte, 1984 , vol. 117, # 5 p. 1994 - 1997
参考文献
Riobe
Annales de Chimie (Cachan, France), 1949 , vol. <12>4, p. 628