3.5-二硝基苯甲酰氯合成路线 (共 144 条)
反应条件
in dichloromethane Refluxing under anaerobic conditions.;
参考文献
Asthana, Anju; Srivastava, Ramesh C.
Journal of Organometallic Chemistry, 1989 , vol. 366, p. 281 - 286
参考文献
Severin,T. et al.
Chemische Berichte, 1969 , vol. 102, p. 3909 - 3914
参考文献
Fronza, Giovanni; Fuganti, Claudio; Grasselli, Piero; Servi, Stefano
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 2086 - 2089
反应条件
in diethyl ether
room temp., 2-4 h; column chromy. (silica gel, CH2Cl2), crystn. (CH2Cl2/n-hexane); elem. anal.;
参考文献
El-Hinnawi, Mahmoud A.; Al-Ajlouni, Ahmad M.; AbuNasser, Jamilah S.; Powell, Anne K.; Vahrenkamp, H.
Journal of Organometallic Chemistry, 1989 , vol. 359, p. 79 - 86
反应条件
pyridine in tetrahydrofuran
0.333333 h; Heating;
参考文献
Feldman, Ken S.; Liu, Yanze; Saunders, Joe C.; Masters, Katherine M.; Campbell, Robert F.
Heterocycles, 2001 , vol. 55, # 8 p. 1527 - 1554
参考文献
Drake; McVey
Journal of Organic Chemistry, 1939 , vol. 4, p. 464,468
反应条件
pyridine
Ambient temperature; Yield given;
参考文献
Fukuzawa, Shin-Ichi; Furuya, Hideki; Tsuchimoto, Teruhisa
Tetrahedron, 1996 , vol. 52, # 6 p. 1953 - 1960
参考文献
Cavier; Gayral; Guillaumel; et al.
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 6 p. 539 - 543
反应条件
1: tetralin / 170 °C
2: nitric acid / -15 °C
View Scheme
参考文献
van Horssen
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 245,251
参考文献
Grummitt; Buck; Joseph
Journal of the American Chemical Society, 1945 , vol. 67, p. 693