1,2-二氯-4-硝基苯合成路线 (共 148 条)
参考文献
Barry et al.
Pr. Irish Acad., 1950 , vol. 53 B, p. 61,67, 82
参考文献
van Duin
Recueil des Travaux Chimiques des Pays-Bas, 1932 , vol. 51, p. 878,879
参考文献
Gupton, John T.; Wysong, Ernest; Norman, Bryan; Hertel, George; Idoux, John P.
Synthetic Communications, 1985 , vol. 15, p. 43 - 52
参考文献
van Loon,A. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1960 , vol. 79, p. 977 - 1001
反应条件
1: (i) aq. NaOH, Na2S2, (ii) /BRN= 635994/
2: Fe, aq. HCl, CuCl2
View Scheme
参考文献
Novello,F.C. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 965 - 970
反应条件
(i) Na, toluene, (ii) /BRN= 1818163/; Multistep reaction;
参考文献
Rondestvedt,C.S.
Journal of Organic Chemistry, 1977 , vol. 42, # 10 p. 1786 - 1790
反应条件
potassium hydroxide in dimethyl sulfoxide
参考文献
Ishihara Sangyo Kaisha Ltd.
Patent: US4106925 A1, 1978 ;
反应条件
1: 1,2-dichloro-4-nitrobenzene; carbon monoxide; [PPN][Rh(CO)4] in tetrahydrofuran
T=-78°C; Carbonylation; 0.5 h;
2: aniline in tetrahydrofuran
T=20°C; Acylation; 4 h;
参考文献
Ragaini, Fabio; Gallo, Emma; Cenini, Sergio
Journal of Organometallic Chemistry, 2000 , vol. 593-594, p. 109 - 118