反应条件
1.1: tetrahydrofuran / 1 h / -40 - -10 °C 1.2: 69 percent / iodine / tetrahydrofuran / -10 - 20 °C 2.1: 59 percent / tetrabutylammonium fluoride / tetrahydrofuran; isopropyl acetate / 2 h 3.1: 70 percent / trifluoroacetic anhydride; DBU / isopropyl acetate / 14 h / Heating 4.1: 89 percent / CO; 1,10-phenanthroline / palladium(II) acetate / dimethylformamide / 16 h / 80 °C / 775.72 Torr View Scheme
参考文献
Davies, Ian W.; Smitrovich, Jacqueline H.; Sidler, Rick; Qu, Chuanxing; Gresham, Venita; Bazaral, Charles
Tetrahedron, 2005 , vol. 61, # 26 p. 6425 - 6437