反应条件
1.1: bromine; iron / 1.5 h / 80 °C / |Inert atmosphere; |Schlenk technique 2.1: copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine / 1,4-dioxane / 20 h / 20 - 100 °C / |Inert atmosphere; |Schlenk technique 3.1: hydrazine hydrate; anhydrous iron chloride; carbon / water / 80 °C / |Inert atmosphere; |Schlenk technique 4.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C / |Inert atmosphere; |Schlenk technique 4.2: 3.17 h / 0 °C / |Inert atmosphere; |Schlenk technique 5.1: 3 h / |Inert atmosphere; |Schlenk technique; |Reflux View Scheme
参考文献
Liu, Yi-Feng; Wang, Cui-Ling; Bai, Ya-Jun; Han, Ning; Jiao, Jun-Ping; Qi, Xiao-Li
Organic Process Research and Development, 2008 , vol. 12, # 3 p. 490 - 495
