in toluene The mixt. of reagents in toluene was heated at 100°C for 5 d (N2atm.), cooling to room temp.;; filtered, chromd. with petroleum ether; elem. anal.;;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2553 - 2560
in neat (no solvent) under N2, (C8H8TiPhC2Ph)2 and PhC2Ph (13.1 equivs.) heated together at 180°C in closed Schlenk tube for 5 h; extd. with pentane, concd., chromd. (Al2O3 (Act. 2-3), pentane), residue extd. with hexane; UV anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 260, # 2 p. 199 - 206
