Zhun', V. I.; Zhun', A. B.; Vlasenko, S. D.; Belorusskaya, L. A.; Chernyshev, E. A.; Sheludyakov, V. D.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 11 p. 2565 - 2570,2266 - 2270
in methanol
initially Me3SiCl and Me2SnHCl are formed in an equil. process, but this is perturbed by the solvolysis of Me3SiCl and destruction of Me2SnHCl (this can be prevented by maintaining the system at low temp.), no evidence of Me3SiSiMe3 formation observed; (1)H NMR data;
参考文献
Cuthberston, Matthew J.; Wells, Peter R.
Journal of Organometallic Chemistry, 1985 , vol. 287, p. 25 - 38
Davidson, Iain M. T.; Matthews, J. Ioan
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1981 , vol. 77, p. 2277 - 2280
in benzene-d6
Irradiation (UV/VIS); Fe complex and trimethylsilane in C6D6 were photolyzed (black light bulb, emission max. 366 nm) for 3 h; monitored by (1)H-NMR, 4,4'-dimethylbiphenyl as internal standard;
参考文献
Casey,C.P.; Austin,E.
Journal of the American Chemical Society, 1988 , vol. 110, p. 7106
