N-(4-溴苄基)-2-丙烯-1-胺合成路线 （共 6 条）
反应条件
magnesium in methanol
T=20°C; 72 h;
参考文献
Tehrani, Kourosch Abbaspour; NguyenVan, Tuyen; Karikomi, Michinori; Rottiers, Mario; De Kimpe, Norbert
Tetrahedron, 2002 , vol. 58, # 35 p. 7145 - 7152
反应条件
sodium cyanoborohydride in methanol
T=0 - 20°C;
参考文献
Benedetti, Erica; Lomazzi, Michela; Tibiletti, Francesco; Palmisano, Giovanni; Penoni, Andrea; Goddard, Jean-Philippe; Fensterbank, Louis; Malacria, Max
Synthesis, 2012 , vol. 44, # 22 art. no. 6763, p. 3523 - 3533,11
反应条件
1: 90 percent / MgSO4*3H2O / CH2Cl2 / 1 h / 20 °C
2: Br2 / CH2Cl2 / 0.5 h / 0 °C
3: 90 percent / NaBH4 / methanol / 2 h / Heating
4: 70 percent / Mg / methanol / 72 h / 20 °C
View Scheme
参考文献
Tehrani, Kourosch Abbaspour; NguyenVan, Tuyen; Karikomi, Michinori; Rottiers, Mario; De Kimpe, Norbert
Tetrahedron, 2002 , vol. 58, # 35 p. 7145 - 7152
反应条件
1: Br2 / CH2Cl2 / 0.5 h / 0 °C
2: 90 percent / NaBH4 / methanol / 2 h / Heating
3: 70 percent / Mg / methanol / 72 h / 20 °C
View Scheme
参考文献
Tehrani, Kourosch Abbaspour; NguyenVan, Tuyen; Karikomi, Michinori; Rottiers, Mario; De Kimpe, Norbert
Tetrahedron, 2002 , vol. 58, # 35 p. 7145 - 7152
反应条件
in dichloromethane
3 h; Inert atmosphere;
参考文献
MacDonald, Melissa J.; Hesp, Colin R.; Schipper, Derek J.; Pesant, Marc; Beauchemin, Andre M.
Chemistry - A European Journal, 2013 , vol. 19, # 8 p. 2597 - 2601
反应条件
Reducing conditions;
参考文献
Ziyaei-Halimehjani, Azim; Marjani, Katayoun; Ashouri, Akram
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3490 - 3492
