Reid; Ruhoff
Organic Syntheses, 1936 , vol. 16, p. 62
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Adams; Marvel
Journal of the American Chemical Society, 1920 , vol. 42, p. 316
in neat (no solvent) (Ar) to sodium diethyl malonate cooled to -196°C acetyl chloride was added, warmed to room temp.; react. mixt. was taken up in EtOH, ppt. was centrifugated and washed with EtOH; powder X-ray diffraction;
in neat (no solvent) react. at room temp. for 15 h; react. mixt. was taken up in EtOH, ppt. was centrifugated and washed with EtOH; powder X-ray diffraction;
