反应条件
in dichloromethane; acetonitrile Irradiation (UV/VIS); irradiation of Fe-complex with 1.5 equiv. of phosphine (150 W flood lamp, 4 h), cooling, filtration, concn., dissoln. in CH2Cl2, cooling to -10°C, bubbling SO2 through soln. for 2 min, stirring for 30 min, warming to room temp.; solvent removal, chromy. (Al2O3, hexane, then CHCl3), solvent removal (vac.), drying (1 mm Hg, overnight);
参考文献
Patel, Paren P.; Welker, Mark E.
Journal of Organometallic Chemistry, 1997 , vol. 547, # 1 p. 103 - 112