反应条件
1: 1.) NaH / 1.) DME, rt, 2 h, 2.a) rt, 2 h, b) reflux, 30 min
2: 1.) NaH / 1.) THF, rt, 1.5 h, 2.) THF, -20 deg C, 1 h
3: NaIO4 / H2O; methanol
4: 65 percent / trimethylphosphite / toluene / 15 h / Heating
View Scheme
参考文献
Barillier, Daniel; Benhida, Rachid; Vazeux, Michel
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 78, # 1-4 p. 83 - 96
