1: With Sm(pentamethylcyclopentadienyl)2*THF in toluene T=20°C; 2: With 1,3-dimethyl-1,3-diaza-2-boracyclopentane in toluene T=80°C; 18 h; 3: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water Further stages.;
参考文献
Molander, Gary A.; Pfeiffer, Dirk
Organic Letters, 2001 , vol. 3, # 3 p. 361 - 363
hydrogen; dicobalt octacarbonyl; [Ru(CO)3Cl2]2; trimethylhexadecylammonium chloride in toluene T=140°C; 15 h; Product distribution / selectivity;
参考文献
Hitachi Chemical Company, Ltd.; National Institute of Advanced Industrial Science And Technology
Patent: EP2206694 A1, 2010 ;
Location in patent: Page/Page column 5 ;
1: With pyridinium p-toluenesulfonate in 1,2-dichloro-ethane T=80°C; 20 h; 2: With triethylamine in dichloromethane T=20°C; 6 h; 3: With trifluoroacetic acid in methanol; dichloromethane T=140°C; 0.0666667 h; microwave irradiation; Further stages.;
参考文献
Buszek, Keith R.; Brown, Neil
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 3125 - 3128
