zinc(II) tetrahydroborate; silica gel in tetrahydrofuran 24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 15 p. 1881 - 1882
sodium (tert-butylamino)trihydroborate in tetrahydrofuran T=66°C; 65 h; further reducing agent: sodium (dimethylamino)trihydroborat (NaDMAB); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 49, # 13 p. 2438 - 2443