Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 12 p. 2601 - 2605
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2805 - 2809
1: 69 percent / AcOK, H2O / methanol / 2 h / 160 °C 2: 97 percent / H2 / Raney-Ni / ethanol / 1.5 h / 20 °C / 18240 Torr View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 12 p. 2601 - 2605
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2805 - 2809
1: diethylzinc With (3R,4S)-2,5-dimethyl-4-(pyrrolidin-1-yl)hexane-3-thiol in toluene T=20°C; 0.333333 h; 2: cyclohexanecarbaldehyde in toluene T=-20°C; 12 h; Title compound not separated from byproducts;
1: triethylaluminum With titanium(IV) isopropylate; (S)-2-hydroxy-3-phenylpropionic acid in tetrahydrofuran; toluene T=21°C; 4 h; 2: cyclohexanecarbaldehyde in tetrahydrofuran; toluene T=21°C; 4 h; Title compound not separated from byproducts;
