反应条件
1: 24 g / dimethyl sulphate / H2O / 5 h / 80 °C
2: sodium hydroxide, water / 4 h / Heating
3: 70 percent / hydrogen chloride (gas) / 4 h / Heating
4: N-chlorosuccinimide, azobisisobutyronitrile / acetic acid; CCl4 / 60 °C / Irradiation; chlorinated reagent was added during 8 h
View Scheme
参考文献
Clarke, Kenneth; Goulding, John; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1501 - 1505
