反应条件
in neat (no solvent) byproducts: CF3SiBr; under dry N2, in a sealed tube, 60 h at room temp., molar ratio of silane and HBr was 1:1, an other non-volatile product was also formed; fractionated distn. at a low-temp. column, S-compds. were trapped at 143K, SiF4 at 77 K;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 627, # 6 p. 1217 - 1224
