4-苯基-3-丁炔-1-醇合成路线 （共 39 条）
反应条件
4-chloro-phenol; molybdenum carbonyl in octane
16 h; Heating; Yield given;
参考文献
Villemin, Didier; Heroux, Michael; Blot, Virginie
Tetrahedron Letters, 2001 , vol. 42, # 22 p. 3701 - 3703
反应条件
pyridine in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
参考文献
Severa, Lukas; Adriaenssens, Louis; Vavra, Jan; Saman, David; Cisarova, Ivana; Fiedler, Pavel; Teply, Filip
Tetrahedron, 2010 , vol. 66, # 19 p. 3537 - 3552
反应条件
1: 65 percent / pyridine / 1.) 1 h, room temp., 2.) 24 h, refrigerator
2: Na2CO3 / 288 h / 80 °C
3: trifluoromethanesulfonic acid / 3 h
View Scheme
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
trifluorormethanesulfonic acid
3 h;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=20°C; 12 h;
参考文献
Wessig, Pablo; Mueller, Gunnar
Chemical Communications, 2006 , # 43 p. 4524 - 4526
反应条件
1: 1-phenyl-1-butyn-4-ol With COCl2
2: lithium phenylacetylide Further stages.;
参考文献
Wessig, Pablo; Mueller, Gunnar; Pick, Charlotte; Matthes, Annika
Synthesis, 2007 , # 3 p. 464 - 477
反应条件
sodium acetate; pyridinium chlorochromate in dichloromethane
T=20°C; 3 h;
参考文献
Zhang, Yong-Qiang; Zhu, Dao-Yong; Li, Bao-Sheng; Tu, Yong-Qiang; Liu, Ji-Xin; Lu, Yong; Wang, Shao-Hua
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 4167 - 4170
反应条件
trimethylsilyl trifluoromethanesulfonate in diethyl ether
T=20°C; 31 h; Inert atmosphere;
参考文献
Ji, Yeon Park; Ullapu, Punna Reddy; Choo, Hyunah; Jae, Kyun Lee; Min, Sun-Joon; Ae, Nim Pae; Kim, Youseung; Baek, Du-Jong; Yong, Seo Cho
European Journal of Organic Chemistry, 2008 , # 32 p. 5461 - 5469
反应条件
4-chloro-phenol; molybdenum carbonyl in octane
16 h; Heating; Yield given;
参考文献
Villemin, Didier; Cadiot, Paul
Tetrahedron Letters, 1982 , vol. 23, # 49 p. 5139 - 5140
