1: diethyl ether / 0.25 h / 0 °C
2: bis(1,5-cyclooctadiene)nickel (0); diphenylcyclohexyl phosphine; cesium fluoride / 1,4-dioxane / 24 h / 40 °C / |Inert atmosphere; |Glovebox
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参考文献
Maity, Prantik; Shacklady-Mcatee, Danielle M.; Yap, Glenn P. A.; Sirianni, Eric R.; Watson, Mary P.
Journal of the American Chemical Society, 2013 , vol. 135, # 1 p. 280 - 285
1: 87 percent / acetonitrile
2: 91 percent / aq. sodium hydroxide / 0 °C
3: tetrahydrofuran / 12 h / 0 °C
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参考文献
Jemison, Robert W.; Mageswaran, Sivapathasuntharam; Ollis, W. David; Sutherland, Ian O.; Thebtaranonth, Yodhathai
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1154 - 1164