1: With (Ph)2SiH2; silver trifluoromethanesulfonate in tetrahydrofuran T=20°C; 40 h; 2: With hydrogenchloride in tetrahydrofuran; methanol Further stages. Title compound not separated from byproducts.;
参考文献
Pakulski, Marcin M.; Mahato, Sanjit K.; Bosiak, Mariusz J.; Krzeminski, Marek P.; Zaidlewicz, Marek
Tetrahedron Asymmetry, 2012 , vol. 23, # 9 p. 716 - 721
1: triethylamine / CH2Cl2 / 0.67 h / -20 °C 2: 95 percent / diethylaluminum chloride / CH2Cl2 View Scheme
参考文献
Maruoka, Keiji; Miyazaki, Tohru; Ando, Mamoru; Matsumura, Yasushi; Sakane, Soichi; et al.
Journal of the American Chemical Society, 1983 , vol. 105, # 9 p. 2831 - 2843
1: triethylamine / CH2Cl2 / 0.67 h / -20 °C 2: 87 percent / DIBAH / CH2Cl2 / 1.) -78 deg C, 5 min, 2.) 0 deg C View Scheme
参考文献
Maruoka, Keiji; Miyazaki, Tohru; Ando, Mamoru; Matsumura, Yasushi; Sakane, Soichi; et al.
Journal of the American Chemical Society, 1983 , vol. 105, # 9 p. 2831 - 2843
