tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20 - 60°C; 24 h;
参考文献
Reeder, Michael R.; Gleaves, Harold E.; Hoover, Sheree A.; Imbordino, Rick J.; Pangborn, Jeffrey J.
Organic Process Research and Development, 2003 , vol. 7, # 5 p. 696 - 699
1: With magnesium in tetrahydrofuran 1 h; Heating; 2: With N,N-diethylphosphoramidous dichloride in tetrahydrofuran cooling; 3: With hydrogenchloride in tetrahydrofuran T=-10 - 20°C;
1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=25°C; Further stages.;
参考文献
Battace, Ahmed; Feuerstein, Marie; Lemhadri, Mhamed; Zair, Touriya; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2007 , # 19 p. 3122 - 3132
